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Diffusion of water in the aluminophosphates AlPO‐5 is studied using a combination of pulsed field gradient NMR and IR microimaging. The concentration profiles measured by the latter allowed to visualize the process of water sorption and propagation into the crystals of AlPO‐5. The self‐diffusion coefficients obtained by NMR were one order of magnitude higher values compared to corrected ones from...
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