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Metal electrodeposition has recently attracted renewed interest in the context of the design of tailored nanomaterials for various applications, such as, for example, fuel cells and sensors. This work is devoted to the investigation of the kinetics of potential-controlled deposition of Pt, at low (below 10μgcm −2 ) metal loadings, on non-porous carbon supports (glassy carbon and highly oriented...
Metatungstate isopolyanion adsorption on smooth polycrystalline Pt and carbon-supported dispersed platinum in sulfuric acid medium is studied by cyclic voltammetry. Manifestations of both reversible and irreversible adsorption are found, with the features typical for heteropolytungstates of the same Keggin structure. When (NH4)6H2W12O40 is added to sulfuric acid solution, H underpotential deposition...
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