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The vibrational spectra of N-(trifluoromethyl)sulfinylamine, CF 3 NSO and N-(pentafluorsulfanyl)sulfinylamine, SF 5 NSO have been recorded and assigned. According to quantum chemical calculations (B3LYP and MP2 with 6-31G(d) and 6-311+G(df) basis sets) the sterically unfavorable syn (Z-) conformers are 2.6–4.1kcal/mol (CF 3 NSO) and 3.1–4.6kcal/mol (SF 5 NSO) lower...
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