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The disulfides FC(O)SSCF 3 , ClC(O)SSCF 3 and ClC(O)SSCH 3 have been prepared by new synthetic routes. Infrared and Raman spectra have been recorded and assigned. From the vibrational spectra and from the gas electron diffraction experiment it was concluded that FC(O)SSCF 3 exists as a mixture of syn- and anti-conformers (C O synperiplanar/antiperiplanar to S S bond)...
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