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The recently synthesized rhodium complex [Rh{P(C5H9)2(η2‐C5H7)}(Me2HNBH3)2]BArF4 (2), which incorporates two amine‐boranes coordinated to the rhodium center with two different binding modes, namely η1 and η2, has been used to probe whether bis(σ‐amine‐borane) motifs are important in determining the general course of amine‐boranes dehydrocoupling reactions. DFT calculations have been carried out to...
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