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This paper reports the study by NMR spectroscopy and ab initio methods of the structure of 3,4-dimethyl-1-cyanophosphole and its dimer. The dimer presents a P···P interaction of the pnictogen type due to the presence of σ-holes. NMR of the monomer was recorded in CDCl 3 solution while NMR of the dimer corresponds to the solid state (CPMAS) experiments. The 2p J PP spin–spin...
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