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Laser flash photolysis (λexc = 266 nm) of α‐sulfinyl diazo compound 1b results in the formation of two transient phenomena. Transient absorption A (intense, λmax = 275 nm) shows jump‐and‐growth behaviour with a growth lifetime of τ = 2 μs. Transient absorption B (weak, λmax = 415 and 540 nm) decays with a lifetime of τ = 1.8 μs, which suggests that B decays into A. On the basis of a comparison with...
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