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A mild and efficient synthesis of a broad scope of substituted naphtho[1,2‐a]pyrene derivatives was accomplished in good yields using an InCl3/AgNTf2‐mediated two‐fold alkyne benzannulation reaction. HPLC enantiomeric separation was achieved and the interconversion barriers have been determined. The ECD spectra of two derivatives were recorded and interpreted through TD‐DFT calculations. Raman spectra...
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