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An air-stable Lewis acidic binuclear complex of bis(ethylcyclopentadienyl)zirconium perfluorooctanesulfonate (1a) was successfully synthesized by the reaction of (CH 3 CH 2 Cp) 2 ZrCl 2 with C 8 F 17 SO 3 Ag. The complex 1a was characterized by different techniques and found to have the nature of air-stability, water tolerance, thermal-stability,...
We report that solid-phase hydrothiolysis is an efficient method to convert resin-bound peptide thioesters to thioacids in aqueous buffer by using a total PEG-based resin. Also demonstrated is the use of the so-prepared peptide thioacids in chemoselective amide bond formation reactions.
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