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The synthesis of titanium–carboxylate metal–organic frameworks (MOFs) is hampered by the high reactivity of the commonly employed alkoxide precursors. Herein, we present an innovative approach to titanium‐based MOFs by the use of titanocene dichloride to synthesize COK‐69, the first breathing Ti MOF, which is built up from trans‐1,4‐cyclohexanedicarboxylate linkers and an unprecedented [TiIV3(μ3‐O)(O)...
Kleinste Fehler gnadenlos aufgedeckt: Mithilfe von Fluoreszenzmikroskopie sind Defekte in Metall‐organischen Gerüsten erkennbar, die während der Synthese entstehen. Gegenüber gängigen Techniken bietet die konfokale Fluoreszenzmikroskopie den Vorteil einer dreidimensionalen Wiedergabe von einzelnen Einkristallen sowie die erforderliche Empfindlichkeit, um den Beginn einer Defektbildung aufzuzeigen.
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