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Phthalimidine (2,3-dihydro-1H-isoindol-1-one) syntheses in recent years are reviewed primarily for those involving synthetic auxiliary-mediated mild Mannich type condensation reactions.
The details of the synthesis and complexation properties of l-tartrate-derived cyclophane (TCP44), the first totally synthetic host with a chiral hydrophobic cavity, are described. The synthesis employs 1:1 cyclization via a U-shaped precursor containing chiral C 4 units derived from l-tartaric acid. TCP44, soluble in acidic water as an amine salt, displayed a complexation selectivity for...
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