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TiO2 nanoparticles with an average diameter of less than 10 nm were prepared via a non‐hydrolytic sol–gel route in a TiCl4–diisopropyl ether–CH2Cl2 system. After modification with n‐octylphosphonic acid (OPA) to increase their organophilic character, the TiO2 nanoparticles were used for preparation of TiO2/epoxy hybrid films. Characterization by FT‐IR, solid‐state 13C cross‐polarization/magic angle...
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