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Nanoporous palladium powders are synthesized on milligram to gram scales by chemical reduction of tetrachloro complexes by ascorbate in a concentrated aqueous surfactant at temperatures between −20 and 30°C. Particle diameters are approximately 50nm, and each particle is perforated by 3nm pores, as determined by electron tomography. These materials are of potential value for storage of hydrogen isotopes...
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