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The kodaistatins A and C (5a,b) inhibit a step in glucose-metabolism at ∼100 nM concentrations. This makes them potential ‘leads’ in the therapy of diabetes. We elucidated the (S)-configuration of the side-chain stereocenter of kodaistatin A by ozonolysis/reduction. The 13 C NMR shifts of kodaistatin A model cis-11 suggest that the diol moiety in the dihydroxycyclopentanone core of kodaistatin...
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