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Hydrates of the dihydronium salt of the superweak anion B12F122– have been synthesized and structurally characterized. The structure of (H3O)2B12F12·6H2O consists of a cubic close‐packed (CCP) array of B12F122– anions intercalated with nonplanar, infinite networks of O6 rings composed of H3O+ ions and H2O molecules. Similar to other salts of B12F122–, (H3O)2B12F12·6H2O exhibits rapid structural modification,...
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