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Two racemic tetrathiafulvalene‐[2.2]paracyclophane electron donors EDT‐TTF‐[2.2]paracyclophane 1 and (COOMe)2‐TTF‐[2.2]paracyclophane 2 have been synthesized via the phosphite mediated cross coupling strategy. Chiral HPLC allowed the optical resolution of the (RP) and (SP) enantiomers for both compounds. Solid‐state structures of (RP)‐1 and (rac)‐2 have been determined by single crystal X‐ray analysis...
Mixed‐valence dyadic [(TTF)2]+. (TTF=tetrathiafulvalene) species—the elementary building blocks of organic conductors—are usually too weakly associated to be observed in solution, unless covalently bound in dimers or physically constrained into a cage structure. We demonstrate here that a novel chiral tetrathiafulvalene functionalised with two 1,1′‐binaphthol units (1) is able to associate in solution...
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