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The one‐pot reactions between anhydrous zinc acetate, diethyl or di‐n‐propyl sulfite, and tetraalkylammonium iodide (120 °C, 12 h) proceed through sulfur‐centered Arbuzov‐type rearrangement to afford [R14N]2[Zn(OSO2R)4] [R1, R = Et (1); R1 = nBu, R = nPr (2)] bearing alkanesulfonate groups bound to the metal center. The zincate salts 1 and 2 are used as precursors for the synthesis of neutral and...
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