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A new experiment for the measurement of nJ(C,P) coupling constants along the phosphodiester backbone in RNA and DNA based on a quantitative-J HCP experiment is presented. In addition to coupling constants, in which a carbon atom couples to only one phosphorus atom, both the intraresidual 3J(C4′i,Pi) and the sequential 3J(C4′i,Pi+1) for the C4′ resonances that couple to two phosphorus atoms can be...
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