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An efficient and stereodefined process is described for the first preparation of a new prenyl-benzoylfuranone type sesquiterpenoid, (+/-)-3-(2,4-dihydroxybenzoyl)-4,5-dimethyl-5-(4,8-dimethyl-3(E),7(E)-nonadi en-1-yl)tetrahydro-2-furanone. The synthetic strategy is based on nucleophilic addition of organometallic reagents to the functionalized ketoamides elaborated from dihydroxyacetone dimer for...
A novel and efficient asymmetric synthesis of the potent actomyosin ATPase activator, penaresidin B, is described in a short and complete stereoselective manner by featuring the elaboration of the fully functionalized homochiral lactam, which can also be regarded as an advanced intermediate for the synthesis of other azetidine alkaloids.
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