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Recently, a novel photochemical reaction of pseudocycloaddition of nitriles to mixed phosphonium–iodonium ylides 1 was found. Nitriles R1CN give corresponding oxazoles (2) with a high yield, with PhI (3) being a leaving group. The mechanism of the photoinduced cycloaddition of acetonitrile to mixed phosphonium–iodonium ylide 1 was studied by steady‐state and time‐resolved methods with resolution from...
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