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Three compounds are described from reactions of divalent nickel species and bicyclic guanidinate ligands. These compounds encompass a variety of nuclearities with one being triangular and having an hour-glass shape and the formula Ni3(tbn)6·2LiCl, 1, where tbn is a bicyclic guanidinate anion with fused 5/6 membered rings. A dinuclear compound [(η2-Imeth)Ni(μ-tbo)]2Cl2, 2, contains two fused 5/5 membered...
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