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The compound (PPh 4 ) 2 [Fe III (CN) 5 (im)]·2H 2 O (1) together with its 13 C labeled analogue have been synthesized (where im is imidazole) and characterized by UV/Vis, LD, IR, Raman and resonance Raman spectroscopy both in solution, powder and single crystalline form. The low spin state of the metal center, Fe III , was confirmed by MCD, EPR...
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