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The reaction of [Re2(CO)8(MeCN)2] with cyanoethylphosphines affords mono- and disubstituted compounds where the phosphine ligand is κ1(P)-coordinated. When diallylphosphines are used as ligands, the μ:κ3(P,C,C)-coordination through the phosphorus atom and an allyl fragment is observed. The hemilabile behavior of the diallyl(p-methoxyphenyl)phosphine ligand was confirmed via the cleavage of the allyl...
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