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p‐tert‐Butylcalix[4]arene is a bowl‐shaped molecule capable of forming a range of polynuclear metal clusters under different experimental conditions. p‐tert‐Butylcalix[8]arene (TBC[8]) is a significantly more flexible analogue that has previously been shown to form mono‐ and binuclear lanthanide (Ln) metal complexes. The latter (cluster) motif is commonly observed and involves the calixarene adopting...
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