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Three manganese clusters have been synthesised via the reaction of Mn II with cyano(imino(methoxy)methyl)nitrosomethanide (cmnm), obtained from the in situ nucleophilic addition of MeOH to dicyanonitrosomethanide (dcnm). X-ray crystallographic studies show that the complex [Mn II3 (cmnm) 6 ]·MeOH (1) is a linear trinuclear species, with a central octahedral and two outer...
The dicyanonitrosomethanide (dcnm) ligand undergoes an in situ transition metal promoted nucleophilic addition of methanol to a nitrile group to form cyano(imino(methoxy)methyl)nitrosomethanide (cmnm) in the formation of the 3d/4f heterometallic complexes (Me 4 N)[{Ni(cmnm) 3 } 2 Ln(cmnm) 2 ] (1Ln; 1Ln=1La, 1Ce, 1Pr, 1Nd, 1Sm). A change in the counter-ions of the metal...
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