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Colorless crystals of ThSiO4 (huttonite) (1) and (Ca0.5Na0.5)2NaThSi8O20 (2) have been synthesized by the solid-state reactions of ThO2, CaSiO3, and Na2WO4 at 1073K. Green crystals of (Ca0.5Na0.5)2NaUSi8O20 (3) have been synthesized by the solid-state reactions of UO2, CaSiO3, and Na2WO4 at 1003K. All three compounds have been characterized by single-crystal X-ray diffraction. Compound 1 adopts a...
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