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The reaction of the neutral triangular species [Mn 3 O(O 2 CR) 6 L 3 ] (R=Me, Ph, CMe 3 ; L=py) with the tripodal ligands H 3 tmp (1, 1, 1-tris(hydroxymethyl)propane) and H 4 peol (pentaerythritol) affords the enneanuclear complexes [Mn 9 O 7 (O 2 CMe) 11 (tmp)(py) 3 (H 2 O) 2 ] (2); [Mn...
The combination of MnBr 2 ·4H 2 O with tripodal alcohols results in the formation of new octa- and dodecametallic [Mn4IIIMn4II] and [Mn6IIIMn6II] clusters. Their structures describe ‘one-dimensional’ rod-like arrays of six and ten edge-sharing triangles, respectively. Both complexes display S≈0 spin ground states.
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