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VT 1H NMR spectroscopy proved that a non‐dissociative and reversible mesomerization process links the tetranuclear indium(III) complexes meso‐(Δ,Δ,Λ,Λ)(P,P,M,M)‐3 and meso‐(Λ,Λ,Δ,Δ)(M,M,P,P)‐3′. During this process four tandem Bailar twists, resulting in the (Δ)/(Λ) isomerization at the indium centers, and the (P)/(M) inversion of the four coordinating face‐centered, helical ligands (L3)3– are involved...
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