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Single crystals of [Be3(μ3‐O)3(MeCN)6{Be(MeCN)3}3](I)6·4CH3CN (1·4CH3CN) were obtained in low yield by the reaction of beryllium powder with iodine in acetonitrile suspension, which probably result from traces of beryllium oxide containing the applied beryllium metal. The compound 1·4CH3CN forms moisture sensitive, colourless crystal needles, which were characterized by IR spectroscopy and X‐ray diffraction...
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