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The direct formation of a β-alcoxyalcohol from the corresponding olefin was investigated through the study of the oxidation of cyclohexene with hydrogen peroxide, as test reaction, catalysed by commercially available MoO 3 in the presence of alcohols. The formation of the corresponding β-alcoxycyclohexanol was favourable in the order Me>Et> i Pr> t Bu, reaching approximately...
Commercially available molybdenum(VI) compounds, including molybdenum trioxide, were successfully employed as catalyst precursors in the epoxidation of olefins with urea–hydrogen peroxide adduct (UHP) in the ionic liquid 1-butyl-3-methylimidazolium hexafluorophosphate, [C 4 mim][PF 6 ]. After oxidation, the corresponding epoxides were isolated by extraction with diethyl ether. Additionally...
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