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Neutron powder diffraction data were collected on a sample of Ca 2 IrD 5 for five temperatures from 20 to 295 K. At room temperature, the symmetry is face-centered cubic, but between 295 and 275 K a phase transition to body-centered tetragonal symmetry is seen. In the cubic phase, there is a single octahedral D site with 5/6 occupancy and an Ir-D distance of 1.702(3) A. In the tetragonal...
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