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The synthesis of Cr(CO)3‐complexed aromatic nitrones 2 is reported. These new planar‐chiral complexes were fully characterized in solution by 1H and 13C NMR, IR and cyclic voltammetry. Moreover, structural data were obtained from X‐ray structures of nitrones 2b, 2d, 2e and 2f. These analyses converge to give evidence of a favoured anti conformation of ortho‐substituted nitrones, with an unusual N–O...
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