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The syntheses of the first rhombicuboctahedral copper polyhydride complexes [Cu28(H)15(S2CNR)12]PF6 (NR=NnPr2 or aza‐15‐crown‐5) are reported. These complexes were analyzed by single‐crystal X‐ray and one by neutron diffraction. The core of each copper hydride nanoparticle comprises one central interstitial hydride and eight outer‐triangular‐face‐capping hydrides. A further six face‐truncating hydrides...
Dithiolat‐geschützte Kupferhydrid‐Nanocluster die bei Bestrahlung mit Sonnenlicht Wasserstoff freisetzen, wurden von C. W. Liu und Mitarbeiter in ihrer Zuschrift auf S. 7342 ff. hergestellt. Diese Nanocluster wurden mit verschiedenen spektroskopischen Methoden, unter anderem Einkristall‐Neutronenbeugung, untersucht. Die zwiebelartige Struktur weist eine geometrische Anordnung auf, die an eine chinesische...
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