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A structural study of ligand exchange on chalcogen‐passivated copper nanoclusters is far less developed. Herein, we report the synthesis of polyhydrido copper nanoclusters [Cu20H11{Se2P(OiBu)2}9] (2) passivated by Se‐donor ligands via ligand replacement reaction on [Cu20H11{S2P(OiPr)2}9] (1) with NH4[Se2P(OiBu)2]. In parallel to the synthesis of 2, cluster [Cu20H11{S2P(CH2CH2Ph)2}9] (4) was produced...
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