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Irradiation of Cp *2 Nb(η 2 -S 2 )H (Cp * = C 5 Me 5 ) 1a in the presence of Fe(CO) 5 gives the CO-free complex [Cp *2 NbS 2 ] 2 Fe 2a. The core of 2a contains an FeS 4 tetrahedron which is ligated by two niobocene ligands as shown by X-ray diffraction analysis. In the reaction of 1a or Cp x ...
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