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Li18P6N16 was synthesized by reaction of LiPN2 and Li7PN4 at 5.5 GPa and 1273 K employing the multi‐anvil technique. It is the first lithium nitridophosphate obtained by high‐pressure synthesis. Moreover, it is the first example received by reaction of two ternary lithium nitrides. The combination of high‐pressure conditions with a Li3N flux enabled a complete structure determination using single‐crystal...
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