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o‐Carborane was covalently linked to the side chain of a polystyrene polymer by the “click” reaction to provide acarborane‐appended polystyrene polymer. The initial step involved the radical polymerization of p‐chloromethylstyrene with AIBN followed by replacement of the chloro units by azido groups; the final step employed the CuI‐catalyzedHuisgen‐type “click” reaction between the azidomethyl‐appended...
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