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Micro-Raman spectroscopy (MRS) was utilized to investigate the graphitization of diamond particles within a UO2-diamond composite processed by spark plasma sintering (SPS). While pure diamond gives a sharp Raman peak at 1331.6 cm−1, the graphitized diamond shows broad peaks either at 1350 cm−1 (G-peak) or 1580 cm−1 (D-peak). The degree of graphitization was quantified by calculating the area beneath...
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