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An investigation of the low temperature reaction of H 2 Os 3 (CO) 10 with phosphines afforded four novel isomeric derivatives of the H(μ-H)Os 3 (CO) 10 (phosphine) adduct in addition to the previously reported one. Their structures have been suggested on the basis of 1 H, 13 C and 31 P NMR data. They represent the...
The solution structures and the dynamic behavior of the acetonitrile substituted cluster compounds M 3 (CO) 12-x (NCCH 3 ) x (M = Os, x = 1 (1), x = 2 (2); M = Ru, x = 1 (3), x = 2 (4), x = 3 (5)) have been investigated by 13 C NMR spectroscopy. The acetonitrile ligands in 1-5 adopt axial positions. In the bisubstituted derivatives 2 and...
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