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The title compound, [C12H24O6][H3PMo12O40]·22H2O, was synthesized by the self-assembly of 18-crown-6 (abbreviated as C12H24O6 or 18C6) and H3PMo12O40 in the mixed solvent of CH3OH and CH3CN, and was characterized by IR, 1H NMR and X-ray diffraction for the first time. Crystal data: Triclinic, P1̄,a=13.428(3)Å,b=13.557(3)Å,c=14.642(3)Å,α=105.39(3)°, β=90.06(3)°, γ=119.56(5)°, V=2207.5(8)Å3,Z=1,...
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