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A mechanism of the capacity loss in LiMn 2 O 4 was studied by comparison of two types of spinel with different morphologies and specific surface areas (2.9 and 0.8 m 2 g −1 ). The combination of SSCV and in situ XRD techniques shows that the irreversible structural conversion occurs partially in spinel of the low specific surface area during the first Li deintercalation...
The effect of Co⇒Ni substitution on the structural and electrochemical properties of Li x Co 1−y Ni y O 2 (0<x<1, y=l or y=0.8) was studied by a combination of slow scan rate cyclic voltammetry (SSCV) and in-situ XRD techniques. It was shown that LiCo 0.2 Ni 0.8 O 2 exhibits a single phase region upon oxidation up to 4.08 V (Li/Li +...
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