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Polystyrene-polybutadiene-polystyrene triblock copolymers were roll-cast from toluene solutions to form globally oriented films. Microstructural changes following thermal annealing of films with cylindrical and lamellar morphology were monitored using two-dimensional small angle X-ray scattering, transmission electron microscopy and thermomechanical analysis. The microdomains in the unannealed films...
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