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The electrode materials with high rate capability are required to meet the ever‐demanding performance of rechargeable batteries. Herein, sulfur‐doped molybdenum phosphide (S:MoP) is prepared using (thio)urea‐phosphate‐assisted strategy and investigated as anode material for Li‐ and Na‐ion batteries. This approach provides the self‐doping of sulfur in MoP lattice that stabilizes the least stable oxidation...
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