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NiAl hydrotalcites with Ni/Al molar ratios of 2–5 and prepared using CO32−, Cl − , NO3−, or SO42− as a guest inorganic anion, were evaluated for the liquid-phase selective oxidation of a methylene group of ethylbenzene to carbonyl functionality with atmospheric pressure of oxygen as the sole oxidant under solvent-free and mild reaction conditions. Among the different NiAl hydrotalcites, the...
Molybdenum sulfide cluster [Mo 3 S 4 (H 2 O) 9 ] 4+ and nickel–molybdenum bimetallic sulfide cluster [Mo 3 NiS 4 Cl(H 2 O) 9 ] 3+ were incorporated into zeolites NaY, HUSY, NaHβ, Na-mordenite (NaMOR), and KL by aqueous ion exchange. EXAFS data revealed that the structure of the molybdenum sulfide cluster remained virtually...
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