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The photocatalytic activity of phosphonated Re complexes, [Re(2,2′‐bipyridine‐4,4′‐bisphosphonic acid) (CO)3(L)] (ReP; L=3‐picoline or bromide) immobilised on TiO2 nanoparticles is reported. The heterogenised Re catalyst on the semiconductor, ReP–TiO2 hybrid, displays an improvement in CO2 reduction photocatalysis. A high turnover number (TON) of 48 molCO molRe−1 is observed in DMF with the electron...
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