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A precursor for Li3PS4 solid electrolyte was successfully prepared by reaction of Li2S and P2S5 in ethyl acetate. The precursor was composed of Li3PS4 and ethyl acetate in a molar ratio of 1:2, as determined by thermogravimetry-differential thermal analysis (TG-DTA). Upon drying at 160°C, the precursor decomposed to form crystalline Li3PS4 with a high ionic conductivity of 3.3×10−4Scm−1 and low activation...
A suspension of a submicron Li3PS4 (LPS) precursor in dimethyl carbonate was successfully prepared by shaking the mixture of starting materials and dimethyl carbonate with the presence of zirconia balls. LPS precursor formation from Li2S and P2S5 was complete after shaking for 5h. Amorphous LPS was obtained from the precursor by drying at 190°C; the ionic conductivity was 6.4×10−6Scm−1, which is lower...
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