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Zinc oxide (ZnO) nanoparticles containing oxygen vacancies were synthesized by the French process modified with pulsed injection of nitrogen. Zinc vapor was generated by evaporation of zinc foil and carried by a carrier gas to react with co-currently supplied air. During the reaction, nitrogen gas was injected in pulse, perpendicular to the flow direction of both zinc vapor and air. Low partial pressure...
Thermal decomposition of titanium (IV) n-butoxide (TNB) in organic solvents yields nanosized anatase titania without the contamination of other phases. The formation of anatase titania crystals and their phase transformation are investigated by using X-ray diffraction (XRD), SEM, BET techniques. It is suggested that anatase titania synthesized in 1,4-butanediol is the result from direct crystallization...
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