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Fourier‐transform infrared‐spectroscopy (FT‐IR) was used to study the photochemistry of CO‐inhibited Azotobacter vinelandii Mo nitrogenase using visible light at cryogenic temperatures. The FT‐IR difference spectrum of photolyzed hi‐CO at 4 K comprises negative bands at 1973 cm–1 and 1679 cm–1 together with positive bands at 1711 cm–1, 2135 and 2123 cm–1. The negative bands are assigned to a hi‐CO...
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