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Self‐immolative polymers are a special kind of degradable polymers that depolymerize into small molecules through a cascade of reactions upon stimuli‐triggered cleavage of the polymer chain ends. This work reports the design and synthesis of a fluoride‐triggered self‐immolative polyester. A 2,4‐disubstitued 4‐hydroxy butyrate is first confirmed to quickly cyclize in solution to form a γ−butyrolactone...
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