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The mechanisms of energy deposition in matrix-assisted laser desorption/ionization mass spectrometry with infrared lasers (IR-MALDI-MS) have been evaluated in a series of experiments. In a first part, the threshold fluences for the generation of IR-MALDI spectra were determined between 2.7 and 4.0 μm wavelength with an optical parametric oscillator as a tunable laser source for nine solid state and...
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